Structures by: Rosa P.

Total: 105

[Delta-Co3(dpa)4(MeCN)2[As2(Lambda-tart)2]2[TBA]2

C44H38Co3N14,2(C8H4As2O12),2(C16H36N)[solvent]

Srinivasan, AnandiCortijo, MiguelBulicanu, VladimirNaim, AhmadClérac, RodolpheSainctavit, PhilippeRogalev, AndreiWilhelm, FabriceRosa, PatrickHillard, Elizabeth A.

Chemical science (2018) 9, 5 1136-1143

a=20.6668(10)Å   b=20.6668(10)Å   c=16.8568(9)Å

α=90°   β=90°   γ=90°

[Co3(dpa)4(MeCN)2][As2(tart)2] acetonitrile solvate

C44H38Co3N14,C8H4As2O12,2(C2H3N)

Srinivasan, AnandiCortijo, MiguelBulicanu, VladimirNaim, AhmadClérac, RodolpheSainctavit, PhilippeRogalev, AndreiWilhelm, FabriceRosa, PatrickHillard, Elizabeth A.

Chemical science (2018) 9, 5 1136-1143

a=17.794(4)Å   b=19.121(4)Å   c=19.042(4)Å

α=90°   β=116.941(15)°   γ=90°

C44H38Co3N14,2(F6P),C4H10O,C2H3N

C44H38Co3N14,2(F6P),C4H10O,C2H3N

Srinivasan, AnandiCortijo, MiguelBulicanu, VladimirNaim, AhmadClérac, RodolpheSainctavit, PhilippeRogalev, AndreiWilhelm, FabriceRosa, PatrickHillard, Elizabeth A.

Chemical science (2018) 9, 5 1136-1143

a=11.7226(9)Å   b=21.8073(17)Å   c=12.0149(9)Å

α=90°   β=112.115(3)°   γ=90°

[Delta-Co3(dpa)4(MeCN)2[As2(Lambda-tart)2]2[TBA]2

C44H38Co3N14,2(C8H4As2O12),2(C16H36N)[solvent]

Srinivasan, AnandiCortijo, MiguelBulicanu, VladimirNaim, AhmadClérac, RodolpheSainctavit, PhilippeRogalev, AndreiWilhelm, FabriceRosa, PatrickHillard, Elizabeth A.

Chemical science (2018) 9, 5 1136-1143

a=20.6481(10)Å   b=20.6481(10)Å   c=16.8896(9)Å

α=90°   β=90°   γ=90°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1192(7)Å   b=14.5268(9)Å   c=17.0178(10)Å

α=90.00°   β=93.017(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1215(12)Å   b=14.5537(12)Å   c=17.0259(8)Å

α=90.00°   β=92.957(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0070(10)Å   b=14.3798(10)Å   c=16.6543(6)Å

α=90.00°   β=92.812(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0917(6)Å   b=14.1960(9)Å   c=17.1443(10)Å

α=90.00°   β=94.310(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0920(6)Å   b=14.1832(9)Å   c=17.1387(10)Å

α=90.00°   β=94.321(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1117(11)Å   b=14.5148(12)Å   c=17.0110(8)Å

α=90.00°   β=93.032(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0934(6)Å   b=14.2495(9)Å   c=17.1470(10)Å

α=90.00°   β=94.234(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1103(11)Å   b=14.4939(12)Å   c=17.0017(8)Å

α=90.00°   β=93.063(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1196(7)Å   b=14.5444(10)Å   c=17.0230(11)Å

α=90.00°   β=92.966(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0970(6)Å   b=14.3013(9)Å   c=17.1496(11)Å

α=90.00°   β=94.136(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0918(6)Å   b=14.2146(9)Å   c=17.1441(10)Å

α=90.00°   β=94.286(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0940(6)Å   b=14.2636(9)Å   c=17.1499(11)Å

α=90.00°   β=94.206(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0958(6)Å   b=14.2842(9)Å   c=17.1476(11)Å

α=90.00°   β=94.159(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1239(7)Å   b=14.5665(10)Å   c=17.0273(11)Å

α=90.00°   β=92.929(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1034(6)Å   b=14.3594(10)Å   c=17.1456(11)Å

α=90.00°   β=94.006(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0995(6)Å   b=14.3215(10)Å   c=17.1475(11)Å

α=90.00°   β=94.087(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1104(7)Å   b=14.4217(10)Å   c=17.1457(12)Å

α=90.00°   β=93.883(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1158(7)Å   b=14.5070(9)Å   c=17.0102(11)Å

α=90.00°   β=93.051(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1213(7)Å   b=14.5553(10)Å   c=17.0282(11)Å

α=90.00°   β=92.945(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1221(7)Å   b=14.5091(11)Å   c=17.1448(13)Å

α=90.00°   β=93.707(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1005(6)Å   b=14.3391(10)Å   c=17.1470(11)Å

α=90.00°   β=94.050(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1281(7)Å   b=14.5550(11)Å   c=17.1464(13)Å

α=90.00°   β=93.621(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1251(8)Å   b=14.5335(12)Å   c=17.1467(15)Å

α=90.00°   β=93.657(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0920(6)Å   b=14.2288(9)Å   c=17.1508(10)Å

α=90.00°   β=94.277(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1170(7)Å   b=14.4666(10)Å   c=17.1452(12)Å

α=90.00°   β=93.793(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1195(7)Å   b=14.4879(11)Å   c=17.1458(13)Å

α=90.00°   β=93.756(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1300(8)Å   b=14.5806(13)Å   c=17.1485(16)Å

α=90.00°   β=93.558(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1135(7)Å   b=14.4437(10)Å   c=17.1447(12)Å

α=90.00°   β=93.836(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1082(7)Å   b=14.4006(10)Å   c=17.1451(12)Å

α=90.00°   β=93.924(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-zinc(ii)

C38H28N10S2Zn

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1058(7)Å   b=14.3790(10)Å   c=17.1457(12)Å

α=90.00°   β=93.973(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0064(8)Å   b=14.3397(11)Å   c=16.6293(13)Å

α=90.00°   β=92.918(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0068(9)Å   b=14.3500(12)Å   c=16.6364(14)Å

α=90.00°   β=92.859(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=14.9984(9)Å   b=14.3524(10)Å   c=16.6350(6)Å

α=90.00°   β=92.822(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0133(8)Å   b=14.3893(11)Å   c=16.6664(12)Å

α=90.00°   β=92.825(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0070(8)Å   b=14.3657(10)Å   c=16.6511(12)Å

α=90.00°   β=92.856(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0119(11)Å   b=14.3903(11)Å   c=16.6678(8)Å

α=90.00°   β=92.793(4)°   γ=90.00°

C38H28FeN10S2

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0171(9)Å   b=14.3939(12)Å   c=16.6705(14)Å

α=90.00°   β=92.807(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0090(11)Å   b=14.3641(11)Å   c=16.6475(7)Å

α=90.00°   β=92.803(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0534(8)Å   b=14.4184(10)Å   c=16.7682(12)Å

α=90.00°   β=92.865(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0800(7)Å   b=14.4253(9)Å   c=16.8673(11)Å

α=90.00°   β=92.994(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0178(10)Å   b=14.4001(10)Å   c=16.6809(7)Å

α=90.00°   β=92.794(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0821(11)Å   b=14.4302(11)Å   c=16.8916(7)Å

α=90.00°   β=93.026(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0294(11)Å   b=14.4106(11)Å   c=16.7098(7)Å

α=90.00°   β=92.796(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0368(9)Å   b=14.4119(12)Å   c=16.7208(14)Å

α=90.00°   β=92.815(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0266(8)Å   b=14.4078(11)Å   c=16.6985(13)Å

α=90.00°   β=92.813(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0861(11)Å   b=14.4369(11)Å   c=16.9270(7)Å

α=90.00°   β=93.073(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0406(10)Å   b=14.4132(10)Å   c=16.7432(7)Å

α=90.00°   β=92.832(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1046(11)Å   b=14.4631(11)Å   c=16.9754(8)Å

α=90.00°   β=93.103(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0676(7)Å   b=14.4217(10)Å   c=16.8187(11)Å

α=90.00°   β=92.929(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0984(6)Å   b=14.4452(9)Å   c=16.9444(10)Å

α=90.00°   β=93.086(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1045(7)Å   b=14.4584(9)Å   c=16.9678(10)Å

α=90.00°   β=93.103(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1127(7)Å   b=14.4897(9)Å   c=16.9969(10)Å

α=90.00°   β=93.083(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0902(6)Å   b=14.4342(9)Å   c=16.9112(10)Å

α=90.00°   β=93.056(3)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0573(10)Å   b=14.4200(10)Å   c=16.7947(7)Å

α=90.00°   β=92.889(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0961(11)Å   b=14.4493(11)Å   c=16.9550(7)Å

α=90.00°   β=93.099(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1081(7)Å   b=14.4721(9)Å   c=16.9844(11)Å

α=90.00°   β=93.095(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0713(10)Å   b=14.4223(11)Å   c=16.8453(7)Å

α=90.00°   β=92.962(4)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1186(12)Å   b=14.5293(12)Å   c=17.0171(8)Å

α=90.00°   β=93.012(4)°   γ=90.00°

[MBqn2+](BF4)2 Methylbiquinoxen bis tetrafluoroborate

C18H16N4,2(BF4)

Leblanc, NicolasSproules, StephenFink, KarinSanguinet, LionelAlévêque, OlivierLevillain, EricRosa, PatrickPowell, Annie K.

Chem. Sci. (2016) 7, 6 3820

a=7.5470(8)Å   b=7.8860(7)Å   c=8.9920(9)Å

α=66.005(7)°   β=85.305(8)°   γ=83.508(8)°

[CdCl2(MBqn)]

C18H16Cd1Cl2N4

Leblanc, NicolasSproules, StephenFink, KarinSanguinet, LionelAlévêque, OlivierLevillain, EricRosa, PatrickPowell, Annie K.

Chem. Sci. (2016) 7, 6 3820

a=7.4683(5)Å   b=10.4739(7)Å   c=11.3249(8)Å

α=80.150(6)°   β=82.274(5)°   γ=81.982(6)°

C29H27CoN5O,2(BF4)

C29H27CoN5O,2(BF4)

Jeon, Ie-RangCalancea, SergiuPanja, AnangamohanPiñero Cruz, Dalice M.Koumousi, Evangelia S.Dechambenoit, PierreCoulon, ClaudeWattiaux, AlainRosa, PatrickMathonière, CorineClérac, Rodolphe

Chemical Science (2013) 4, 6 2463

a=21.346(5)Å   b=12.362(5)Å   c=12.855(4)Å

α=90.00°   β=120.033(13)°   γ=90.00°

C22H11FeN8,2(C16H36N),6(H2O)

C22H11FeN8,2(C16H36N),6(H2O)

Jeon, Ie-RangCalancea, SergiuPanja, AnangamohanPiñero Cruz, Dalice M.Koumousi, Evangelia S.Dechambenoit, PierreCoulon, ClaudeWattiaux, AlainRosa, PatrickMathonière, CorineClérac, Rodolphe

Chemical Science (2013) 4, 6 2463

a=21.267(2)Å   b=11.4830(13)Å   c=26.049(3)Å

α=90.00°   β=111.875(2)°   γ=90.00°

C22H13FeN8,H2O

C22H13FeN8,H2O

Jeon, Ie-RangCalancea, SergiuPanja, AnangamohanPiñero Cruz, Dalice M.Koumousi, Evangelia S.Dechambenoit, PierreCoulon, ClaudeWattiaux, AlainRosa, PatrickMathonière, CorineClérac, Rodolphe

Chemical Science (2013) 4, 6 2463

a=10.9398(12)Å   b=22.107(3)Å   c=16.8809(19)Å

α=90.00°   β=92.003(6)°   γ=90.00°

2(C51H36CoFeN13),5(CH4O)

2(C51H36CoFeN13),5(CH4O)

Jeon, Ie-RangCalancea, SergiuPanja, AnangamohanPiñero Cruz, Dalice M.Koumousi, Evangelia S.Dechambenoit, PierreCoulon, ClaudeWattiaux, AlainRosa, PatrickMathonière, CorineClérac, Rodolphe

Chemical Science (2013) 4, 6 2463

a=13.5995(10)Å   b=14.2091(10)Å   c=24.9650(19)Å

α=90.00°   β=103.148(3)°   γ=90.00°

2(C51H36CoFeN13),5(CH4O)

2(C51H36CoFeN13),5(CH4O)

Jeon, Ie-RangCalancea, SergiuPanja, AnangamohanPiñero Cruz, Dalice M.Koumousi, Evangelia S.Dechambenoit, PierreCoulon, ClaudeWattiaux, AlainRosa, PatrickMathonière, CorineClérac, Rodolphe

Chemical Science (2013) 4, 6 2463

a=13.6545(15)Å   b=14.3480(17)Å   c=25.328(3)Å

α=90.00°   β=102.313(5)°   γ=90.00°

C14H12Mn1N2O4S1

C14H12Mn1N2O4S1

Grirrane, AbdessamadPastor, AntonioGalindo, AgustínIenco, AndreaMealli, CarloRosa, Patrick

Chemical Communications (Cambridge, United Kingdom) (2003) 4 512-513

a=8.018(3)Å   b=9.104(3)Å   c=10.484(4)Å

α=73.86(2)°   β=72.86(3)°   γ=80.71(3)°

?

C14H20P2S

Rosa, PatrickRicard, LouisMathey, FrançoisFloch, Pascal Le

Chemical Communications (1999) 6 537

a=9.861(1)Å   b=15.219(2)Å   c=10.715(1)Å

α=90°   β=110.95(1)°   γ=90°

(Dy3),(C5F6O2H)3,(C20O4N4H28),(CHCl3)

(Dy3),(C5F6O2H)3,(C20O4N4H28),(CHCl3)

Bernot, KevinPointillart, FabriceRosa, PatrickEtienne, MaelSessoli, RobertaGatteschi, Dante

Chemical communications (Cambridge, England) (2010) 46, 35 6458-6460

a=12.1870(4)Å   b=13.1630(4)Å   c=31.5810(11)Å

α=90.0010(14)°   β=79.8310(15)°   γ=76.7410(14)°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=15.670(7)Å   b=8.175(10)Å   c=18.648(7)Å

α=90.00°   β=110.21(5)°   γ=90.00°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=14.925(9)Å   b=7.861(5)Å   c=18.28(2)Å

α=90.00°   β=111.02(10)°   γ=90.00°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=15.186(19)Å   b=7.967(3)Å   c=18.57(3)Å

α=90.00°   β=111.53(18)°   γ=90.00°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=14.80(2)Å   b=7.69(2)Å   c=18.15(11)Å

α=91.0(5)°   β=112.0(4)°   γ=89.4(2)°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=14.849(6)Å   b=7.823(4)Å   c=18.233(16)Å

α=90.00°   β=111.47(7)°   γ=90.00°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Shepherd, Helena J.Rosa, PatrickVendier, LaureCasati, NicolaLétard, Jean-FrançoisBousseksou, AzzedineGuionneau, PhilippeMolnár, Gábor

Physical chemistry chemical physics : PCCP (2012) 14, 15 5265-5271

a=15.409(11)Å   b=8.078(7)Å   c=18.56(3)Å

α=90.00°   β=110.54(13)°   γ=90.00°

C38H34Fe2N16O2S4

C38H34Fe2N16O2S4

Kaiba, A.Shepherd, H. J.Fedaoui, D.Rosa, P.Goeta, A. E.Rebbani, N.Létard, J FGuionneau, P.

Dalton transactions (Cambridge, England : 2003) (2010) 39, 11 2910-2918

a=30.958(3)Å   b=16.109(1)Å   c=19.613(2)Å

α=90.000°   β=117.500(5)°   γ=90.000°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Kaiba, A.Shepherd, H. J.Fedaoui, D.Rosa, P.Goeta, A. E.Rebbani, N.Létard, J FGuionneau, P.

Dalton transactions (Cambridge, England : 2003) (2010) 39, 11 2910-2918

a=15.8910(7)Å   b=17.3839(7)Å   c=18.3423(8)Å

α=72.0480(10)°   β=90.0010(10)°   γ=62.7980(10)°

C36H26Fe2N16S4,2(CH4O)

C36H26Fe2N16S4,2(CH4O)

Kaiba, A.Shepherd, H. J.Fedaoui, D.Rosa, P.Goeta, A. E.Rebbani, N.Létard, J FGuionneau, P.

Dalton transactions (Cambridge, England : 2003) (2010) 39, 11 2910-2918

a=16.0463(14)Å   b=17.3628(16)Å   c=18.5495(17)Å

α=72.1780(10)°   β=89.9320(10)°   γ=62.5580(10)°

C14H12Mn1N2O4S1

C14H12Mn1N2O4S1

Grirrane, AbdessamadPastor, AntonioGalindo, AgustínIenco, AndreaMealli, CarloRosa, Patrick

Chemical Communications (Cambridge, United Kingdom) (2003) 4 512-513

a=8.018(3)Å   b=9.104(3)Å   c=10.484(4)Å

α=73.86(2)°   β=72.86(3)°   γ=80.71(3)°

C82H69Cl20Co8N16O27P2

C82H69Cl20Co8N16O27P2

R. WinpennyMadeleine HelliwellStuart LangleyPatrick RosaRoberta SessoliW.Wernsdorfer

Chemical Communications (2005)

a=20.551(2)Å   b=21.853(2)Å   c=25.909(3)Å

α=90.00°   β=104.703(2)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.0091(9)Å   b=14.3725(12)Å   c=16.6495(14)Å

α=90.00°   β=92.839(5)°   γ=90.00°

Bis(N-(2-Pyridylmethylene)-4-(phenylazo)aniline)-diisothiocyanato-iron(ii)

C38H28FeN10S2

Lakhloufi, S.Lemée-Cailleau, M HChastanet, G.Rosa, P.Daro, N.Guionneau, P.

Physical chemistry chemical physics : PCCP (2016) 18, 40 28307-28315

a=15.1063(11)Å   b=14.4809(11)Å   c=16.9914(8)Å

α=90.00°   β=93.085(4)°   γ=90.00°

C30H48LiN2O5P2

C30H48LiN2O5P2

Sylvie ChouaHelena SidorenkovaThéo BerclazMichel GeoffroyPatrick RosaNicolas MézaillesLouis RicardFrançois MatheyPascal Le Floch

Journal of the American Chemical Society (2000) 122, 12227-12234

a=11.5316(6)Å   b=11.5497(5)Å   c=13.0148(4)Å

α=74.998(3)°   β=74.883(3)°   γ=72.182(2)°

C76H132Fe4O18

C76H132Fe4O18

Stefania AccorsiAnne-Laure BarraAndrea CaneschiGuillaume ChastanetAndrea CorniaAntonio C. FabrettiDante GatteschiCecilia MortalòEmiliano OlivieriFrancesca ParentiPatrick RosaRoberta SessoliLorenzo SoraceWolfgang WernsdorferLaura Zobbi

Journal of the American Chemical Society (2006) 128, 4742-4755

a=16.1893(12)Å   b=16.1893(12)Å   c=56.712(10)Å

α=90.00°   β=90.00°   γ=120.00°

Fe4Ph

Fe4C86H136O18,C4H10O

Stefania AccorsiAnne-Laure BarraAndrea CaneschiGuillaume ChastanetAndrea CorniaAntonio C. FabrettiDante GatteschiCecilia MortalòEmiliano OlivieriFrancesca ParentiPatrick RosaRoberta SessoliLorenzo SoraceWolfgang WernsdorferLaura Zobbi

Journal of the American Chemical Society (2006) 128, 4742-4755

a=19.357(3)Å   b=21.617(2)Å   c=24.740(4)Å

α=90.00°   β=109.050(10)°   γ=90.00°

C80H144Fe4O18

C80H144Fe4O18

Stefania AccorsiAnne-Laure BarraAndrea CaneschiGuillaume ChastanetAndrea CorniaAntonio C. FabrettiDante GatteschiCecilia MortalòEmiliano OlivieriFrancesca ParentiPatrick RosaRoberta SessoliLorenzo SoraceWolfgang WernsdorferLaura Zobbi

Journal of the American Chemical Society (2006) 128, 4742-4755

a=16.4332(2)Å   b=16.4332(2)Å   c=57.6317(9)Å

α=90.00°   β=90.00°   γ=120.00°

Bis (cobalt(II) phenyl(carboxymethyl)phosphinate aqua), aqua

C16H18Co2O10P2,H2O

Stefano MidolliniAnnabella OrlandiniPatrick RosaLorenzo Sorace

Inorganic Chemistry (2005) 44, 2060-2066

a=23.185(9)Å   b=9.2020(10)Å   c=9.706(4)Å

α=90°   β=89.94(5)°   γ=90°

C34H32Mn2O6P4

C34H32Mn2O6P4

František HartlTaasje MahabiersingPascal Le FlochFrancois MatheyLouis RicardPatrick RosaStanislav Záliš

Inorganic Chemistry (2003) 42, 4442-4455

a=22.3415(9)Å   b=10.6463(3)Å   c=16.0877(7)Å

α=90.0000(10)°   β=118.7330(10)°   γ=90.0000(10)°

C17H16BrMnO3P2

C17H16BrMnO3P2

František HartlTaasje MahabiersingPascal Le FlochFrancois MatheyLouis RicardPatrick RosaStanislav Záliš

Inorganic Chemistry (2003) 42, 4442-4455

a=15.1080(5)Å   b=12.5770(6)Å   c=10.0060(8)Å

α=90.00°   β=99.591(3)°   γ=90.00°

C25H36MnNaO5P2

C25H36MnNaO5P2

František HartlTaasje MahabiersingPascal Le FlochFrancois MatheyLouis RicardPatrick RosaStanislav Záliš

Inorganic Chemistry (2003) 42, 4442-4455

a=9.024(5)Å   b=10.130(5)Å   c=15.833(5)Å

α=96.830(5)°   β=90.140(5)°   γ=103.770(5)°

?

C46H56OP6W

Patrick RosaLouis RicardPascal Le FlochFrançois MatheyGjergji SiniOdile Eisenstein

Inorganic Chemistry (1998) 37, 3154-3158

a=24.815(3)Å   b=14.700(2)Å   c=16.754(2)Å

α=90°   β=127.57(1)°   γ=90°

C56H58Cl4Co2N2P4S2,2(CH2Cl2)

C56H58Cl4Co2N2P4S2,2(CH2Cl2)

Fliedel, ChristopheRosa, VitorVileno, BertrandParizel, NathalieChoua, SylvieGourlaouen, ChristopheRosa, PatrickTurek, PhilippeBraunstein, Pierre

Inorganic chemistry (2016) 55, 9 4183-4198

a=11.7798(5)Å   b=15.9919(9)Å   c=16.8204(9)Å

α=93.135(2)°   β=95.456(3)°   γ=98.989(3)°

C4H12Cl3CoNS

C4H12Cl3CoNS

Fliedel, ChristopheRosa, VitorVileno, BertrandParizel, NathalieChoua, SylvieGourlaouen, ChristopheRosa, PatrickTurek, PhilippeBraunstein, Pierre

Inorganic chemistry (2016) 55, 9 4183-4198

a=10.5383(4)Å   b=11.1199(5)Å   c=18.1015(9)Å

α=90.00°   β=90.00°   γ=90.00°

C56H58ClCoN2P4S2,F6P,CH2Cl2

C56H58ClCoN2P4S2,F6P,CH2Cl2

Fliedel, ChristopheRosa, VitorVileno, BertrandParizel, NathalieChoua, SylvieGourlaouen, ChristopheRosa, PatrickTurek, PhilippeBraunstein, Pierre

Inorganic chemistry (2016) 55, 9 4183-4198

a=44.4062(17)Å   b=13.0561(6)Å   c=22.6438(5)Å

α=90°   β=106.959(2)°   γ=90°

2(C7H10NS),Cl4Co

2(C7H10NS),Cl4Co

Fliedel, ChristopheRosa, VitorVileno, BertrandParizel, NathalieChoua, SylvieGourlaouen, ChristopheRosa, PatrickTurek, PhilippeBraunstein, Pierre

Inorganic chemistry (2016) 55, 9 4183-4198

a=6.9440(3)Å   b=12.4765(5)Å   c=12.7558(4)Å

α=69.658(2)°   β=82.329(2)°   γ=86.360(2)°

C56H58Cl5Co2N2P4S2

C56H58Cl5Co2N2P4S2

Fliedel, ChristopheRosa, VitorVileno, BertrandParizel, NathalieChoua, SylvieGourlaouen, ChristopheRosa, PatrickTurek, PhilippeBraunstein, Pierre

Inorganic chemistry (2016) 55, 9 4183-4198

a=12.1774(4)Å   b=15.9750(4)Å   c=16.2155(5)Å

α=98.646(2)°   β=110.634(2)°   γ=90.728(2)°